Difficulties measuring salt level accurately

TheHarold

5000 Club Member
View Badges
Joined
Oct 3, 2015
Messages
5,145
Reaction score
8,759
Rating - 0%
0   0   0
I love my Milwaukee digital refractometer and will never change to anything else. Reads perfectly every time, and every few months I calibrate it with a 0ppt solution and certify accuracy with a 35ppt solution.

Just needs 1 drop of water

 

homer1475

Figuring out the hobby one coral at a time.
View Badges
Joined
Apr 24, 2018
Messages
11,799
Reaction score
18,826
Location
Way upstate NY
Rating - 0%
0   0   0
Also please note that the temp of refractometer will affect the reading so it should be close to tank water temp and not 10-20 degrees cooler.

If your refractometer says ATC on it, the water temp and instrument temp does not matter. The reading curve is automatically compensating for.

Seriously read the instructions on an ATC refractometer or watch the BRS video on them. They all say the same thing regarding instruments that have ATC.
 

Super Fly

Valuable Member
View Badges
Joined
Apr 19, 2018
Messages
1,454
Reaction score
1,103
Rating - 0%
0   0   0
If your refractometer says ATC on it, the water temp and instrument temp does not matter. The reading curve is automatically compensating for.

Seriously read the instructions on an ATC refractometer or watch the BRS video on them. They all say the same thing regarding instruments that have ATC.
even though mine says ATC, it's definitely not ATC. Like I said, if left in basement, mine will give different reading vs when unit is similar temp to tank water. Bought it from Amazon as ATC w label but definitely not ATC.
 

birdy123

New Member
View Badges
Joined
Jan 13, 2020
Messages
7
Reaction score
2
Rating - 0%
0   0   0
Just found this on tropic marine website in regard to readings of refractometers.....
ts taken a while, but I am now happy with the measurements.

I believe the following points should be highlighted to customers with this device:
1. You will NOT get reproducible results if you use too much RO water to clean between each measurement (also only need 3- 4 drops of solution, no more). I found it is best to use 2 lens cloths - one to wipe sample away and the other to final clean no rinsing with RO at all.
2. You will get apparent drift in calibration if you DO NOT leave the refrac out in the open in the room that measurement will be taken for some time for temperature of refrac to equilibrate. I was storing refrac in its box in a cupboard in the room where I was taking readings, and this was sufficient to cause daily discrepancies in readings.
 

Quietman

2500 Club Member
View Badges
Joined
May 14, 2017
Messages
3,272
Reaction score
10,877
Location
Indiana - born and bred
Rating - 0%
0   0   0
As a general rule with all test equipment you need to calibrate for range expected to see or a max and min that covers the range.

Best pH are 4.0, 10.0, 7.0 (last being optional, but I do it). Salinity - 35.0 and make sure you allow temps to equalize (if calibration liquid is colder storage), I also use known standards periodically for all my titration test kits to verify my "calibrated" eye balls.

And repeated open and closed fluids can lose calibration accuracy on certain parameters as well.
 
OP
OP
T

the_chef_pierre

Active Member
View Badges
Joined
Jan 22, 2020
Messages
431
Reaction score
110
Rating - 0%
0   0   0
Hey everyone. So my lfs was actually able to measure my salinity and they read it at around 1.024 (which is close to the 1.025 i find when calibrating with RODI water as opposed to the 1.020 reading i was getting using the calibration fluid). They told me that I could be experiencing this problem due to my calibration fluid possibly being off. I only just purchased it but theres no visible expiration date on the bottle. Wondering if this was maybe just sitting on their shelves for too long. Either way, I plan on sticking with my original calibration with the RODI water since this is what the manual for my refractometer states and gives me the closest reading to what the lfs found. Thanks again guys for all the help and support with this.
 

Waters

"...in perfect isolation, here behind my wall."
View Badges
Joined
Nov 5, 2013
Messages
8,036
Reaction score
17,514
Location
Mentor, OH
Rating - 0%
0   0   0
I love my Milwaukee digital refractometer and will never change to anything else. Reads perfectly every time, and every few months I calibrate it with a 0ppt solution and certify accuracy with a 35ppt solution.

Just needs 1 drop of water

I wish mine was that accurate lol. I calibrate before every use (as instructed) and it will still sometimes read incorrectly (normally high). I then re-calibrate and it reads correctly. Do you wait for the temp of the water to stop moving before you test? Maybe I need to stop calibrating lol.
 

fcmatt

Well-Known Member
View Badges
Joined
Jul 4, 2016
Messages
765
Reaction score
944
Location
MA
Rating - 0%
0   0   0
You bought calibration fluid from a local fish store? I would not recommend that if that is the case.... my lfs sells a couple test kits that are expired from 2012 for example....

You have to buy that stuff from a high volume seller.
 

TheHarold

5000 Club Member
View Badges
Joined
Oct 3, 2015
Messages
5,145
Reaction score
8,759
Rating - 0%
0   0   0
I wish mine was that accurate lol. I calibrate before every use (as instructed) and it will still sometimes read incorrectly (normally high). I then re-calibrate and it reads correctly. Do you wait for the temp of the water to stop moving before you test? Maybe I need to stop calibrating lol.

The way you describe it sounds like you are leaving salt water on it, which evaporated to form salt and give a false (yet true) high reading of your sample. That is why your first test is abnormally high, yet the second one works (since excess salt is gone).
 

Thespammailaccount

2500 Club Member
View Badges
Joined
Jan 3, 2020
Messages
4,274
Reaction score
15,567
Location
Houston
Rating - 0%
0   0   0
The Hanna salinity is good for checking newly mixed saltwater I will is it on occasion to check the temp. The Milwaukee digital salinity is the instrument I trust
 

madweazl

2500 Club Member
View Badges
Joined
Sep 19, 2016
Messages
4,110
Reaction score
5,092
Location
Virginia
Rating - 0%
0   0   0
There are a couple easy ways to get a sanity check. First, what salt are you using? When you mix it up to what you believe is 1.026 (or whatever your target is), what are your alkalinity, calcium, and magnesium levels? If they're lower than what the salt manufacturers suggests, your salinity is probably low (you need to look at all three).

A sure fire method is to use Randy's calibration standard. I'd trust my dog testing the aquarium more than the LFS.

Also, calibrate every single time you use the device.
 

Uncle99

7500 Club Member
View Badges
Joined
Jul 22, 2018
Messages
9,025
Reaction score
13,265
Location
Province of Ontario
Rating - 0%
0   0   0
It is more important to provide a stable salinity than whether it’s a point, up or down.
My swing arm says 1.024
My calibrated refractometer says 1.025
Lab testing confirms, it’s actually 1.027
Look like it’s been 1.027 for three years instead of 1.025
E903C8B7-6E73-423F-8B32-8CD1ABB2E3B8.jpeg

no losses and everyone happy
 

High pressure shells: Do you look for signs of stress in the invertebrates in your reef tank?

  • I regularly look for signs of invertebrate stress in my reef tank.

    Votes: 34 31.2%
  • I occasionally look for signs of invertebrate stress in my reef tank.

    Votes: 26 23.9%
  • I rarely look for signs of invertebrate stress in my reef tank.

    Votes: 21 19.3%
  • I never look for signs of invertebrate stress in my reef tank.

    Votes: 28 25.7%
  • Other.

    Votes: 0 0.0%
Back
Top