Calibrating refractometer

Hi all,
So from Randy's article, RO should be 1ppt?
I am wondering if my 35ppt solution is old and no longer accurate. I have left the bottle uncapped overnight a few times over the last 3 plus years.
When I tested RO, my refractometer read far below the zero line. Thoughts?
Thanks in advance.
 
I would buy or make some new calibration fluid. Even one night w/ the cap left off will be enough to throw off your readings. think about how much water evaporates from your tank each day. About 1% right? Say that happens 5 times... now your calibration fluid is at 36.75 ppt. cross checking w/ RO water will not confirm your refractometer is calibrated correctly.
 

WHAT KIND OF SUBSTRATE ARE YOU RUNNING ON YOUR TANK?

  • Bare bottom

    Votes: 3 20.0%
  • A shallow bed of fine sand

    Votes: 3 20.0%
  • A shallow bed of coarser sand

    Votes: 3 20.0%
  • A deep sand bed

    Votes: 2 13.3%
  • Mixed substrate or varying sand depth

    Votes: 4 26.7%
  • Some other substrate (posted in the comments)

    Votes: 0 0.0%
  • I don’t have a reef tank yet

    Votes: 0 0.0%
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