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Hi. @Randy Holmes-Farley and I had a discussion few weeks ago, and I promised investigate in which way zinc dose is crucial or not for nitrate tests. Here is my test, summarized in a small article.
Randy or someone responsible for the forum , feel free to relocate this to the article threads, or if you find it more appropriate somewhere else:-)
Its a very easy study, and a follow up would be interesting to do with higher nitrate concentrations , as I think the "break point" where zinc dose is crucial depends also on nitrate conc. A nitrate test is probably designed to have an excess amount of zinc for all nitrate values up to the tests "roof". Up to that value an overdose of zinc will have no negative effect on accuracy, but a too low dose will have when the "new" zinc dose is that low so its lower the "roof" below your true nitrate value. Where that limit is hard to know, so its always most safe to be careful when dosing the zinc powder.
Jonas
Randy or someone responsible for the forum , feel free to relocate this to the article threads, or if you find it more appropriate somewhere else:-)
Its a very easy study, and a follow up would be interesting to do with higher nitrate concentrations , as I think the "break point" where zinc dose is crucial depends also on nitrate conc. A nitrate test is probably designed to have an excess amount of zinc for all nitrate values up to the tests "roof". Up to that value an overdose of zinc will have no negative effect on accuracy, but a too low dose will have when the "new" zinc dose is that low so its lower the "roof" below your true nitrate value. Where that limit is hard to know, so its always most safe to be careful when dosing the zinc powder.
Jonas
