ICP Results Help

jimb090

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Hi, can anyone help me with these results that I just got back? I'm confused at the salinity/sodium and chloride readings.

Firstly, I've been using a refractometer, calibrated regularly and consistently sitting at 1.024/1.025 S.G. these results would indicated a S.G. of 1.022. are refractometers that inaccurate? Or is mine a dud? Is there any more accurate way or reading this or recommendations for a decent one?

Secondly, if my sodium and chloride concentrations are good, how is the salinity so far off? Won't increasing the salt concentration send these too high?

Thanks

Jim

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redfishbluefish

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How are you calibrating your refractometer? If you're using RO/DI you can easily get inaccurate results. Best to use a calibration solution as close to the values you wish to measure. If not purchasing the solution, you can make your own. HERE's Randy's recipe.
 

rtparty

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Do NOT use any pre made calibration solutions. They are all junk. Make your own with some Morton’s table salt and RO water

You want 35ppt or 1.0264sg seawater
 
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jimb090

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How are you calibrating your refractometer? If you're using RO/DI you can easily get inaccurate results. Best to use a calibration solution as close to the values you wish to measure. If not purchasing the solution, you can make your own. HERE's Randy's recipe.
That's awesome, thanks a lot. I have been using RODI. Any ideas on the sodium and chloride being in range?
 

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